Investigation of the effect of boriding on the wear behaviour of AISI 1050 carbon steel

In this study, AISI 1050 carbon steel samples were boronized with the powder pack boriding technique at 875°C for 2, 4 and 6 hours using Ekabor 2 boriding powder. The boride layer thicknesses obtained with the boriding time increased and after 2, 4 and 6 hours of boriding, a 30.6, 40.0 and 71.8 µm boride layer, predominantly composed of Fe2B phase, was obtained. Boride layers were formed in tooth-like morphology. Thanks to this boride layer, the surface hardness of the substrate was improved 6.2-6.4 times and a maximum surface hardness of 1543.8 HV was reached. With the Daimler-Benz Rockwell-C adhesion tests, it was determined that the adhesion quality of the boride layer was generally at the HF1 level. With the boriding carried out, the specific wear loss of AISI 1050 steel was reduced from 421.25 mm3/Nm x10-6 to 17.67 mm3/Nm x10-6, and the wear resistance was increased approximately 24 times.

Keywords:

AISI 1050, Boriding, Fe2B Wear,

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1. Hernandez-Ramirez, E.J., A. Guevara-Morales, U. Figueroa-Lopez and I. Campos-Silva, Wear resistance of diffusion annealed borided AISI 1018 steel, Materials Letters, 2020. 277: 128297.
2. Genel, K., Boriding kinetics of H13 steel, Vacuum, 2006. 80: p. 451-457.
3. Er, U. and B. Par, Wear of plowshare components in SAE 950C steel surface hardened by powder boriding, Wear, 2006. 261: p. 251-255.
4. Çavdar, U. and E. Atik, Properties of boronized, carbonitrided and steamed ıron-based compact, Materials Testing, 2014. 56(2): p. 126-130.
5. Altintaş, A., Y. Sarigün and U. Çavdar Effect of Ekabor 2 powder on the mechanical properties of pure iron powder metal compacts. Revista de Metalurgia, 2016. 52(3): e073.
6. Akshay, A.J. and S.S. Hosmani, Pack-boriding of AISI 4140 steel: boriding mechanism and the role of container design, Materials and Manufacturing Processes, 2014. 29: p. 1062-1072.
7. Turkmen, I., E. Yalamac and M. Keddam, Investigation of tribological behaviour and diffusion model of Fe2B layer formed by pack-boriding on SAE 1020 steel, Surface and Coatings Technology, 2019. 377: 124888.
8. Ulutan, M., M.M. Yildirim, O.N. Celik and S. Buytoz, Tribological properties of borided AISI 4140 steel with the powder pack-boriding method, Tribology Letters, 2010. 38: p. 231-239.
9. Turkmen, I. and E. Yalamac, Effect of alternative boriding mixtures on boride layer and tribological behaviour of borided SAE 1020 steel, Metals and Materials International, 2022. 28: p. 1114-1128.
10. Arslan, D. and S. Akgün, Mechanical characterization of pack-boronized AISI 4140 and AISI H13 steels, International Advanced Researches and Engineering Journal, 2021. 5(1): p. 61-71.
11. Kartal, G., O.L. Eryilmaz, G. Krumdick, A. Erdemir and S. Timur, Kinetics of electrochemical boriding of low carbon steel, Applied Surface Science, 2011. 257: p. 6928-6934.
12. Genel, K., I. Ozbek and C. Bindal, Kinetics of boriding of AISI W1 steel, Materials and Science Engineering, 2003. A347: p. 311-314.
13. Sen, S., I. Ozbek, U. Sen and C. Bindal, Mechanical behaviour of borides formed on borided cold work tool steel, Surface and Coatings Technology, 2001. 135: p. 173-177.
14. Arslan, M., A.C. Ok, G.K. Sireli and S. Timur, Investigation on stuructural and tribological properties of borided gear steel after phase homogenization, Surface and Coatings Technology, 2022. 429: 127967.
15. Martini, C., G. Palombarini, G. Poli and D. Prandstraller, Sliding and abrasive wear behaviour of boride coatings,Wear, 2004. 256: p. 608-613.
16. Liu, Y., X. Liu, C. Lai, J. Ma, X. Meng, L. Zhang, G. Xu, Y. Lu, H. Li, J. Wang and S. Chen, Boriding of tungsten by the powder-pack process: Phase formation, growthkinetics and enhanced neutron shielding, International Journal of Refratory Metals and Hard Materials, 2023, 110: 10649.
17. Günen, A., M. Keddam, A. Erdoğan and M.S. Karakaş, Pack‑Boriding of Monel 400: Microstructural Characterization and Boriding Kinetics, Metals and Materials International, 2022, 28: 1851-1863.
18. Yildiz, I., Surface Characterization and Boriding of Nickel and Cobalt Alloys, Protection of Metals and Physical Chemistry of Surfaces, 2022, 58: 772–778.
19. Kaner, S., Y. Kaplan, Ö., Pamuk and S. Aksöz, Production and Tribological Investigation of Cr Borides by Boriding of Powder Metallurgy Pure Chromium Surface, Journal of Materials Engineering and Performance, (2022). https://doi.org/10.1007/s11665-022-07195-4.
20. Kanca, Y., Microstructural characterization and dry sliding wear behavior of boride layers grown on Invar-36 superalloy, Surface and Coating Technology, 2022, 449: 128973.
21. Garcia-Leon, R.A., J. Martinez-Trinidad, I. Campos-Silva, U. Figueroa-Lopez and A. Guevara-Morales, Development of tribological maps on borided AISI 316L stainless steel under ball-on-flat wet sliding conditions, Tribology International, 2021. 163: 107161.
22. Selcuk, B., R. Ipek and M.B. Karamis, A study on friction and wear behaviour of carburized, carbonitrided and borided AISI 1020 and 5115 steels, Journal of Materials Processing Technology, 2003. 141: p. 189-196.
23. Ueda, N., T. Mizukoshi, K. Demizu, T. Sone, A. Ikenaga and M. Kawamoto, Borıding of nickel by the powder-pack method, Surface and Coatings Technology, 2000. 126: p. 25-30.
24. Taktak, S., Tribological behaviour of borided bearing steels at elevated temperatures, Surface and Coatings Technology, 2006. 201: p. 2230-2239.
25. Ipek Ayvaz, S. and I. Aydin, Tribological and adhesion properties of microwave-assisted borided AISI 316L steel, Materials Testing, 2022. 64: p. 249-259.
26. Ipek Ayvaz, S. and I. Aydin, Effect of the microwave heating on diffusion kinetics and mechanical properties of borides in AISI 316l, Transactions of the Indian Instute of Metals, 2020. 73: p. 2635-2644.
27. Carrera-Espinoza, R., , U. Figueroa-Lopez, J. Martinez-Trinidad, I. Campos-Silva, E. Hernandez-Sanchez and A. Motallebzadeh, Tribological behavior of borided AISI 1018 steel under linear reciprocating sliding conditions, Wear, 2016. 362-363: p. 1-7.
28. Sezgin, C.T. and F. Hayat, The effects of boriding process on tribological properties and corrosive behavior of a novel high manganese steel, Journal of Materials Processing Tech., 2022, 300: 117421.
29. Medvedovski, E., Formation of corrosion-resistant thermal diffusion boride coatings, Advanced Engineering Materials, 2016. 18: p. 11-33.
30. Krelling, A.P., F. Teixeira, C.E. da Costa, E.A.S. Almeida, B. Zappelino and J.C.G. Milan, Microabrasive wear behavior of borided steel abraded by SiO2 particles, Journal of Materials Research and Technology, 2019. 8: p. 766-776.
31. Atik, E., U. Yunker and C. Meric, The effects of conventional heat treatment and boriding on abrasive wear and corrosion of SAE 1010, SAE 1040, D2 and 304 steels, Tribology International, 2003. 36: p. 155-161.
32. Petrova, R. and N. Suwattananont, Surface modification of ferrous alloys with boron, Journal of Electronic Materials, 2005. 34: p. 575-582.
33. Boztepe, M.H. and M. Bayramoglu, Optimization of process parameter of boronized AISI 1050 steel using the taguchi analysis, The 17th International Conference on Machine Design and Production, 2016. Bursa: p. 1-11.
34. Milinovic, A., S. Brod, D. Krumes, I. Kladaric, S. Klaric and S. Aracic, An investigation of boride layers growth kinetics on C15 steel, 16th International Research/Expert Conference “Trends in the Development of Machinery and Associated Technology, 2012. Dubai: p. 135-138.
35. Vidakis, N., A. Antoniadis and N. Bilalis, The VDI 3198 indentation test evaluation of a reliable qualitative control for layered compounds, Journal of Materials Processing Technology, 2003. 481: p. 143–144.
36. Küçükkurt, M., Borlanmış AISI M35 ve AISI M42 Çeliklerinin Karakterizasyobu ve Aşınma Davranışlarının İncelenmesi, 2015. Afyon Kocatepe Üniversitesi: Turkey. p. 112.
37. Gunes, İ. and I. Yıldız, Investigation of Adhesion and Tribological Behavior of Borided AISI 310 Stainless Steel, Revistamateria, 2016. 21: p. 61-71.
38. Garcia-Leon, R.A., J. Martinez-Trinidad, R. Zepeda-Bautista, I. Campos-Silva, A. Guevara-Morales, J. Martinez-Londono and J. Barbosa-Saldana, Dry sliding wear test on borided AISI 316L stainless steel under ball-on-falt configuration: a statistical analysis, Tribology International, 2021. 157: 106885.
39. Soydan, Y., S. Köksal, A. Demirer and V. Çelik, Sliding Friction and Wear Behavior of Pack-Boronized AISI 1050, 4140, and 8620 Steels, Tribology Transactions, 2008. 51: p. 74-81.