Vedat AKTAŞ, Ali MARACI, Hacali NECEFOĞLU, Füreya Elif ÖZBEK

Metal(II) 4-Etilbenzoatların Karışık-Ligand Komplekslerinin Sentezi ve Karakterizasyonu

Bu çalışmada Cu(II), Co(II), Ni(II), Pb(II), Mn(II) ve Zn(II) 4-etilbenzoatların nikotinamid/N,N’- dietilnikotinamid ligandları ile kompleksleri sentezlenmiştir. Komplekslerin yapılarını aydınlatmak için elementel analiz, IR, UV-Vis, 1 H ve 13 C NMR spektroskopisi yöntemleri kullanılmıştır. Sentezlenen komplekslerin termik özelliklerine bakıldığında su ligandı içeren komplekslerde ilk bozunma basamağında su molekülleri yapıdan ayrılmaktadır. Devam eden basamaklarda organik ligandlar tamamen veya kısmen bozunmaya uğramaktadır. Komplekslerin nihai termal bozunma ürünleri uygun gelen metal veya metal oksittir

Anahtar Kelimeler:

“Geçiş Metalleri”, “4- Etilbenzoik Asit”, “Benzoat”, “Nikotinamid”, “N, N’- dietilnikotinamid”

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