Demir esaslı toz metal parçaların sinterleme ile birleştirilmesi

Bu çalışmada demir esaslı tozların ham ve ön sinterlenmiş halde mekanik geçme sonrası sinterleme ilebirleştirilmesi incelenmiştir. Deneylerde presleme basıncı olarak 600 MPa kullanılmış ve sinterleme işlemleriendogaz ortamında ve indirgeyici gaz karışımında (%90$N _2$ + %10$H _2$) 1120˚C’de 45 dakika süre ile yapılmıştır.Demir esaslı tozların (Fe-%0,6P, Fe-%0,6P-%2Cu, Fe-%0,6P-%3Cu-%0,4C) ham halde ve sinterlenmiş haldemekanik özellikleri ölçülmüştür. Sinterleme ile birleştirme işlemlerinde burç-pelet geometrisi kullanılmıştır.Demir esaslı tozlardan preslenerek hazırlanan burç (Fe-%0,6P, Fe-%0,6P-%2Cu) ve pelet (Fe-%0,6P-%3Cu- %0,4C) numuneler ham ve ön sinterlenmiş halde mekanik geçme sonrası sinterlenerek birleştirilmiş ve bağdayanım değerleri ölçülmüştür. Ham halde sinterleme ile birleştirilen burç-pelet toz metal parçalarınınarayüzeyleri optik ve taramalı elektron mikroskobu ile incelenmiştir. Çalışma sonucunda ham halde mekanikolarak geçirilen parçaların sinterleme ile birleştirme işlemlerinin yeterli düzeyde bağ dayanımı sağladığıbulunmuştur.

Joining of iron based powder metallurgy parts with sintering

In this study, joining of iron based green and pre-sintered powder metal parts by sintering was examined.Samples were pressed at 600 MPa and sintered at 1120ºC for 45 minutes under reducing (%90$N _2$ + %10$H _2$) andendogas atmospheres. Mechanical properties of iron based powder samples (Fe-%0.6P, Fe-%0.6P-%2Cu, Fe- %0.6P-%3Cu-%0.4C) were measured under green and sintered conditions. In joining with sintering experimentsring-pellet geometry was utilized. Green and pre-sintered ring (Fe-%0.6P, Fe-%0.6P-%2Cu) and pellet (Fe- %0.6P-%3Cu-%0.4C) samples were joined by sintering and their bonding strengths were measured. Theinterface formed after sinter joining was examined with optical and scanning electron microscopy. The studyshow that green parts can be joined by sintering without an appreciable loss in bonding strength.

___

  • 1. Hamill, J.A., Joining of Ferrous P/M Materials - Principles and Case Studies, The International Journal of Powder Metallurgy, 37(7), 41-45, 2001.
  • 2. Fillabi, G., Simchi, A., Kokabi, H., Effect of Iron Particle Size on the Diffusion Bonding of Fe-5%Cu Powder Compact to Wrought Carbon Steels, Materials and Design, 29 (2), 411-417, 2008.
  • 3. T.Tabata, S.Masaki, K.Kitagawa, Y.Matsuoka, K.Minami, Fabrication of Composite Parts by Sinter Bonding, The International Journal of Powder Metallurgy, 27 (3), 265-273, 1991.
  • 4. T.Tabata, S.Masaki, H.Suzuki ve Q.Zhu, Bond Strength of Sinter Bonded Composite Preforms, The International Journal of Powder Metallurgy, 25(1), 37-41,1989.
  • 5. C.Çetiner, İ.Uslan, S.Sarıtaş, Toz Metal Bronz Yatağın Düşük Karbonlu Çeliğe Difüzyon Kaynağında Mikroyapısal Tespitler, 3. Uluslararası Toz Metal Konferansı, 1322- 1330, 2002.
  • 6. K.Asaka and T.Hayasaka, Diffusion Bonding Method to Assemble Green Compacts During Sintering, Metal Powder Report, 39, 347-350, 1984.
  • 7. T.Pieczonka and J.Kazior, Sinter-Bonding of Iron Based Compacts Containing P and Cu, Materials Science Forum 534, 633-636, 2007.
  • 8. Akatsu, H., Iijima M., Direct Diffusion Bonding Technique for Ferrous P/M Parts. Modern Developments in Powder Metallurgy, 16, 195- 208, 1985.
  • 9. Vyal, E., Laptev, M., Use of certain binders to increase the strength of green compacts, Powder Metallurgy and Metal Ceramics, 44, 614-618, 2005.
  • 10. A.Aksoy, R.Ünal, Sıkıştırma Basıncı ve Yağlayıcı Miktarının Demir Tozlarının Ham Mukavemetine Etkisinin Araştırılması. 10. Denizli Malzeme Sempozyumu ve Sergisi, 2004.
  • 11. Simchi, A., Effects of Lubrication Procedure on the Consolidation, Sintering and Microstructural Features of Powder Compacts, Materials and Design, 24, 585-594, 2003.
  • 12. Lund, J.,Origins of Green Strength in Iron P/M Compacts, The International Journal of Powder Metallurgy and Powder Technology, 18(2), 117-127, 1982.
  • 13. Phadke, B., Relationship Between Transverse Rupture Strength and Hardness of P/M Fe-Cu Alloys, The International Journal of Powder Metallurgy and Powder Technology, 17(1), 37-43, 1981.
  • 14. Kohno, T., Koczak, M.J., Rajagopalan, V., Nishino Y., Sintering Improvements in Strength and Dimensional Control Utilizing Eutectic Phosphide Additions in Iron-Copper-Carbon Alloys, Modern Developments in Powder Metallurgy, 15, 521-540, 1985.
  • 15. ASM Handbook, Vol. 7, Powder Metallurgy, ASM International, USA, s.1107, 1998.
  • 16. German, R.M., Toz Metalurjisi ve Parçacıklı Malzeme İşlemleri, Editörler: S.Sarıtaş, M.Türker, N.Durlu, Ankara: Türk Toz Metalurjisi Derneği Yayınları, 2007.
  • 17. Lawcock, R.L., Davies, T.J., Effect of Carbon on Dimensional and Microstructural Characteristics of Fe-Cu Compacts During Sintering, Powder Metallurgy, 33 (2), 147-150, 1990.
  • 18. Wang, F.,W., Effect of Alloying Elements and Processing Factors on the Microstructure and Hardness of Sintered and Induction-Hardened Fe- C-Cu Alloys, Materials Science and Engineering A, 402, 92-97, 2005.