TERMAL KARARLILIĞI ARTTIRILMIŞ DEMİR ESASLI FERRİTİK ÇELİK TOZLARININ SICAK PRES VE SICAK EKSTRÜZYON (ECAE) YÖNTEMLERİ İLE KONSOLİDASYONU

Bilyeli değirmenler ile üretilen yüksek mukavemetli tozların konsolidasyonunda temel hedef mekanik özelliklerinde önemli bir kayıp olmadan bu tozların birleştirilerek porozite içermeyen ürüne dönüştürülebilmesidir. Son yıllarda yapılan araştırmalar sıcak ekstrüzyon ile yüksek kayma ve basınca maruz bırakılan tozların porozite içermeden, teorik yoğunluklarında birleştirilebileceğini göstermiştir. Bu çalışmada sıcak presleme ve yüksek sıcaklıklarda çok geçişli eş kanallı açısal ekstrüzyon (ECAE - equal channel angular extrusion) teknikleri kullanılarak nano-kristalin Fe-Ni-Zr tozlarından konsolide edilmiş ferritik alaşımların üretimi araştırılmıştır. Elde edilen sonuçlar sıcak presleme metodu ile teorik yoğunluğa ulaşılamadığını, ancak sıcak ekstrüzyon yöntemi ile yapısında porozite içermeyen ve teorik yoğunlukta malzeme üretilebileceğini göstermiştir. Konsolidasyon sonucunda mikroyapıda mikrometre seviyelerine ulaşan tane büyümesi gözlenmesine rağmen üretilen bu çeliklerin sertliği 4-6 GPa civarındadır.

CONSOLIDATION OF THERMALLY STABILIZED FE BASED FERRITIC STEELS VIA HOT PRESSING AND HOT EXTRUSION (ECAE)

The key characteristic of ball-milled powders consolidation process is to achieve densification and particle bonding without degradation in mechanical properties. Recent demonstrations of novel processing methods involving temperature, high shear and high pressure have shown promise for bonding high strength particulate materials. In this study, we report the ability of multi-pass high temperature equal channel angular extrusion (ECAE) and hot pressing to produce fully dense and well-bonded bulk Ferritic alloys from nanocrystalline FeNi-Zr powders. Subsequent microstructural characterizations indicate full consolidation via hot extrusion with grain growth to micron sizes. The consolidated alloys demonstrate an extremely high strength (4-6 GPa) at room temperature.

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