Experimental Investigation of Refractive Index Measurement of Common Solvents and Aqueous Solutions in the Infrared Wavelengths

Experimental Investigation of Refractive Index Measurement of Common Solvents and Aqueous Solutions in the Infrared Wavelengths

We proposed and experimentally demonstrated a fast and simple technique to measure refractive index of liquids. A commercial Optical Time-Domain Reflectometer (OTDR) was implemented for interrogating sensor tips from a remote location. The system uses Fresnel reflected light from standard single mode fiber tips as sensing points without requiring any chemical coating, delicate fiber components, and/or sophisticated architecture at the sensor head. We reported new measurements of refractive indices of common solvents and solutions at both 1550 nm and 1625 nm. The precision of the proposed measurement system was found to be in the order of 10-4. The experimental results have been validated by the way of theoretical calculations.

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  • J. Oelhafen, T. Mayr, F. Dorner, K. Moutzouris, J. Roths, K. Drechsler, “Fiber Optic Measurement System for Fresnel Reflection Sensing: Calibration, Uncertainty, and Exemplary Application in Temperature-Modulated Isothermal Polymer Curing”, Journal of Lightwave Technology, Vol.36, No.4, February 2018, pp.939 - 945.
  • G. An, X. Hao, S. Li, X. Yan, X. Zhang, “D-shaped photonic crystal fiber refractive index sensor based on surface plasmon resonance”, Applied Optics, Vol.56, No.24, 2017, pp.6988-6992.
  • I.D. Villar, J.L. Cruz, A.B. Socorro, S. Diaz, J.M. Corres, F.J. Arregui, I.R. Matias, “Monitoring the Etching Process in LPFGs towards Development of Highly Sensitive Sensors”, Proceedings, Vol.1, No.4, 2017, pp.331-334.
  • K. Yüksel, “Optical fiber sensor system for remote and multi-point refractive index measurement”, Sensors and Actuators A: Physical, Vol.250, 2016, pp.29-34.
  • R. C. Weast, S. M. Selby (ed), Handbook of Chemistry and Physics, (48th edition), CRC Handbook of Chemistry and Physics Press, 1968.
  • C.-B. Kim, C.-B. Su, “Measurement of the refractive index of liquids at 1.3 and 1.5 micron using a fibre optic Fresnel ratio meter”, Measurement Science and Technology, Vol.15, No.9, 2004, pp.1683-1686.
  • A. Basgumus, F.E. Durak, A. Altuncu, G. Yilmaz, “A universal and stable all-fiber refractive index sensor system”, IEEE Photonics Technology Letters, Vol.28, No.2, 2015, pp.171-174
  • W. Xu, X.G. Huang, J.S. Pan, “Simple fiber-optic refractive index sen-sor based on Fresnel reflection and optical switch”, IEEE Sensors Journal, Vol.13, No.5, 2013, pp.1571-1574.
  • C.-L. Zhao, J. Li, S. Zhang, Z. Zhang, S. Jin, “Simple Fresnel reflection-based optical fiber sensor for multipoint refractive index measurement using an AWG”, Photonics Technology Letters, Vol.25, No.6, 2013, pp.606-608.
  • R. Selvas-Aguilar, A. Castillo-Guzman, L. Cortez-Gonzalez, et al., “Noncontact Optical Fiber Sensor for Measuring the Refractive Index of Liquids” Journal of Sensors, Vol.2016, Article ID 3475782, 2016, 6 pages.
  • C.-H. Yeh, C.-W. Chow, J.-Y. Sung, P.-C. Wu, W.-T. Whang, F.-G. Tseng, “Measurement of organic chemical refractive indexes using an optical time-domain reflectometer”, Sensors, Vol.12, No.1, 2012, pp.481-488.
  • J.-Y. Yuan, C.-L. Zhao, M. Ye, J. Kang, Z. Zhang, S.-Z. Jin. “A Fresnel reflection-based optical fiber sensor system for remote refractive index measurement using OTDR”, Photonic Sensors, Vol.4, No.1, March 2014, pp. 48-52.
  • O.V. Butov, K.M. Golant, A.L. Tomashuk, M.J.N. van Stralen, A.H.E. Breuls, “Refractive index dispersion of doped silica for fiber optics”, Optics Communications, Vol.213, 2002, pp.301-308.
  • Y. Kang, Calculations and Measurements of Raman Gain Coefficients of Different Fiber Types, MSc Thesis, Virginia Polytechnic Institute and State University, 2002.
  • J.E. Saunders, C. Sanders, H. Chen, H.-P. Loock, “Refractive indices of common solvents and solutions at 1550 nm”, Applied Optics, Vol.55, No.4, 2016, pp.947-953.
  • J.-H. Chen, X.-G. Huang, W.-X. He, J. Tao, “A parallel-multipoint fi-ber-optic temperature sensor based on Fresnel reflection”, Optics & Laser Technology, Vol.43, No.8, 2011, pp.1424-1427
  • H. Apriyanto, G. Ravet, O.D. Bernal, M. Cattoen, H.C. Seat, V. Chavagnac, F. Surre, J.H. Sharp, “Comprehensive Modeling of Multimode Fiber Sensors for Refractive Index Measurement and Experimental Validation”, Scientific Reports, Vol.8, Article number: 5912, 2018