Amberlit XAD-4 Polimerinin Biyosorbent Katkı Malzemesi Badem Kabuğu Kullanılarak Sulu Çözeltiden Cd Giderilmesi

Bu çalışmada, biyosorbent olarak badem kabuğu ile immobilize edilmiş amberlit XAD-4 polimerinin üzerine Cd(II) iyonlarının katı faz özütleme yöntemi ile zenginleştirilme şartları araştırıldı. Bunun yanında, geri kazanım verimi üzerine ortamın pH etkisi, elüent türü ve derişimi, çözelti akış hızı, çözelti hacminin etkisi, tuz etkisi, kolonun tekrarlanabilirliği, çevre örneklerine ve sertifikalı referans maddeye uygulanması araştırılmıştır. Önerilen yöntem ile Cd için 10 kat zenginleşme sağlanmıştır. Optimum şartlarda, % 95 güven seviyesinde Cd geri kazanım verimi % 98,87 ± 3,85 olarak bulunmuştur. Ayrıca % 95 güven seviyesinde, 3 tekrar deneyi için % bağıl standart sapma değeri Cd için % 3,21 olarak bulunmuştur.

The Removal of Cd From Aqueous Solution Using Sorbents Almont Shell Immobilized On Amberlite XAD-4

In this study; statistical process control is being used on spinwelding machine process. All parameters that used on process control is tested with various type of experiments and effect of these parameters to the capability is analysed. Mini-tap part-cabality analyses, pull-of tests of samples, leaking test, shock test, burst test, visual and optic mıcroscope controls of crosscut samples are examined. As a result of all detailed analyses; special appropriate parameters for machine are defined and with statistical process control - errorproof works(Poka-Yoke, sensor) process is kept under control and ensure its continuity. With this conclusion scrap parts ratio is kept in minimum level in this spinwelding machine.

Kaynakça

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Kaynak Göster