Studies on Mononuclear Chelates Derived from Substituted Schiff Base Ligands (Part 4): Synthesis and Characterization of a New 5-Hydroxysalicyliden-P-Aminoacetophenoneoxime and Its Complexes with Co(II), Ni(II), Cu(II) and Zn(II)

5-Hydroxysalicyliden-p-aminoacetophenoneoxime (LH) was synthesized starting from p-aminoacetophenoneoxime and 5-hydroxysalicylaldehyde. Complexes of this ligand with Co+2, Ni+2, Cu+2 and Zn+2 salts were prepared. With this ligand, complexes were synthesized using Co+2, Ni+2, Cu+2 and Zn+2 salt with a metal:ligand ratio of 1:2. Their structures were elucidated on the basis of elemental analyses, IR, 1H- and 13C-NMR, electronic spectra, magnetic susceptibility measurements, molar conductivity and thermogravimetric analyses.

Studies on Mononuclear Chelates Derived from Substituted Schiff Base Ligands (Part 4): Synthesis and Characterization of a New 5-Hydroxysalicyliden-P-Aminoacetophenoneoxime and Its Complexes with Co(II), Ni(II), Cu(II) and Zn(II)

5-Hydroxysalicyliden-p-aminoacetophenoneoxime (LH) was synthesized starting from p-aminoacetophenoneoxime and 5-hydroxysalicylaldehyde. Complexes of this ligand with Co+2, Ni+2, Cu+2 and Zn+2 salts were prepared. With this ligand, complexes were synthesized using Co+2, Ni+2, Cu+2 and Zn+2 salt with a metal:ligand ratio of 1:2. Their structures were elucidated on the basis of elemental analyses, IR, 1H- and 13C-NMR, electronic spectra, magnetic susceptibility measurements, molar conductivity and thermogravimetric analyses.

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Turkish Journal of Chemistry-Cover
  • ISSN: 1300-0527
  • Yayın Aralığı: 6
  • Yayıncı: TÜBİTAK
Sayıdaki Diğer Makaleler

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Design and Characterization of Amino and Chloro Functionalized Rhombohedral Silsesquioxanes

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Synthesis of Novel Proponohydrazides and Their Hydrolysis Reactions

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Studies on Mononuclear Chelates Derived from Substituted Schiff Base Ligands (Part 4): Synthesis and Characterization of a New 5-Hydroxysalicyliden-P-Aminoacetophenoneoxime and Its Complexes with Co(II), Ni(II), Cu(II) and Zn(II)

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Determination of Cadmium, Copper, Iron, Manganese, Lead and Zinc in Lichens and Botanic Samples by Electrothermal and Flame Atomic Absorption Spectrometry

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Anodic Stripping Voltammetric Behavior of Mercury in Chloride Medium and its Determination at a Gold Film Electrode

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O-Galloyl Flavonoids from Geranium pyrenaicum and Their in vitro Antileishmanial Activity

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Proton conduction in PVPA-benzimidazole hybrid electrolytes

Ayhan BOZKURT, Fatma SEVİL

Studies an mononuclear chelates derived from substituted Schiff base ligands (Part 4):Synthesis and characterization of a new 5-hydroxysalicyliden-P-aminoacetophenoneoxime and its complexes with Co(II),Ni(II),Cu(II) and Zn(II)

Mehmet KAYA, Erdal CANPOLAT

Synthesis of Isomorphous Prototypic [CrFe2O(AcO)6(TEP)3]Cl and [CrFe2O(AcO)6(TMP)3]Cl As Oxo-Centered Hetero Tri-Nuclear Carboxylate Complexes

Massoud RAFIZADEH, Reza TAYEBEE, Vahid AMANI