ESRA ALTINTIĞ, M Emre HİŞİR, Hüseyin ALTUNDAĞ

Determination of Cr, Cu, Fe, Ni, Pb and Zn by ICP-OES in mushroom samples from Sakarya, Turkey

Russula cyanoxantha, Russula delica, Lactarius salmonicolor, Lactarius deliciosus, Pleurotus eryngii, Pleurotus ostreatus, Agaricus bisporus, Suillus luteus, Pleurotus spp and Boletus edulis were collected from Sakarya-Turkey respectively. Also canned food in the form of the Pleurotus eryngii, Pleurotus ostreatus, and Lactarius salmonicolor mushrooms were used for the examination. Trace metal concentrations found in these mushrooms were determined inductively using coupled plasma optic emission spectrometry microwave processes. The results were obtained for (Cr) 0.3-26.65, (Cu) 17.38-132.75, (Fe) 26.3-225.40, (Ni) 2.57-39.28, (Pb) 11.52-185.20, and (Zn) 22.86-126.84 mg/kg. The accuracy of the method was checked by the standard reference material; tea leaves (INCY-TL-1) and tomato leaves (1573a).

Türkiye, Sakarya’dan toplanan mantar numunelerindeki Cr, Cu, Fe, Ni, Pb ve Zn ICP-OES ile tayini

Bu çalışma’da Türkiye’nin Sakarya ilinden Russula cyanoxantha, Russula delica, Lactarius salmonicolor, Lactarius deliciosus, karakulak, Pleurotus ostreatus, Agaricus bisporus, Suillus luteus, Pleurotus spp, orman mantarları ayrı ayrı toplanmıştır. Ayrıca Malgadın, Pleurotus ostreatus, Lactarius salmonicolor mantarlarının konserve türleri alınmıştır. Bu mantarların eser metal konsantrasyonları mikrodalga işleminden sonra indüktif eşleşmiş plazma optik emisyon spektroskopisi (ICP-OES) ile tespit edilmiştir. Sonuçlar (Cr) için 0,3-26,65, (Cu) için 17,38-132,75, (Fe) için 26,3- 225,40, (Ni) için 2,57-39,28, (Pb) için 11,52-185,20, (Zn) için 22,86-126,84 mg/kg olarak tespit edilmiştir. Prosedürün doğruluğu (INCY-TL-1) kodlu çay yaprakları ve (1573a) kodlu domates yaprakları sertifikalı referans malzeme ile doğrulanmıştır.

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