Synthesis and Structural Characterization of N2S2O2 Type Dimeric Schiff Base
– A interesting hexadentate N2S2O2 donor dimeric Schiff base ligand, L2HA(2-(-(2-(2-(2-(-2-hydroxybenzylideneamino)phenyl)disulfanyl)phenylimino) methyl)phenol),was synthesized by the condensation of 2 – aminothiophenol and salicylaldehyde under the argon atmosphere. Structural investigations on the ligand have been made based on spectral data.The ligand was characterized by FT-IR, UV-vis, 1H and 13C NMR spectroscopy.L2HA was isolated and their structures were determined by X – ray crystal structure analysis
___
- A. A. Soliman, G. G. Mohamed, Thermochimica Acta, Vol:421, (2004) 151-159.
- A. A. Soliman, W. Linert, Monatshefte für Chemie, Vol:138, (2007) 175-189.
- S. Durmus, A. Atahan, M. Zengin,Spectrochimica Acta Part A, Vol:84, (2011) 1–5.
- A. H. Kianfar, M. Bahramianb, H. R. Khavasic, Spectrochimica Acta Part A, Vol:94, (2012) 302– 307.
- M. Gupta Bhowon, S. Jhaumeer-Laulloo, N. Soukhee, A. Allibacus, V. Shiboo,Journal of Coordination Chemistry, Vol:60, (2007) 1335–1343.
- H. Keypour, A. Hossein Jamshidi, M. Rezaeivala, L. Valencia,Polyhedron, Vol:52, (2013) 872–878.
- H. Khanmohammadi, F. Khodam, Journal of Molecular Liquids, Vol:177, (2013) 198–203.
- A. Başoğlu, S. Parlayan, M. Ocak, H. Alp, H. Kantekin, M. Özdemir, Ü. Ocak, Polyhedron, Vol:28, (2009) 1115–1120.
- V. Kumar Guptaa, A.K. Singha, M.R. Ganjalic, P. Norouzic, F. Faridbodc, Naveen Mergua, Sensors and Actuators B, Vol:182, (2013) 642– 651.
- A. Shokrollahia, A. Abbaspourb, M. Ghaedia, A. Naghashian Haghighia, A.H. Kianfara, M. Ranjbara, Talanta, Vol:84, (2011) 34–41.
- M. Nath, S. Goyal, Met. Based Drugs, Vol:2, (1995) 297.
- R. Singh, N. K. Kaushik, Spectrochimica Acta A, Vol:65, (2006) 950-954.
- M. Behpour ⇑, S.M. Ghoreishi, N. Mohammadi, M. Salavati-Niasari, Corrosion Science Vol:53, (2011) 3380–3387.
- M. Behpour, S.M. Ghoreishi, N. Mohammadi, N. Soltani, M. Salavati-Niasari, Corrosion Science, Vol:52, (2010) 4046–4057.
- Yi-Ping Tonga, Yan-Wen Lin, Spectrochimica Acta Part A Vol:78, (2011) 809–817.
- ISSN: 1304-7981
- Yayın Aralığı: Yılda 3 Sayı
- Başlangıç: 2012
- Yayıncı: Tokat Gaziosmanpaşa Üniversitesi