Triazines have proved of great interest, academic as well as industrialwit- hin the last two decades. Since hoxamethylmelamine is starting material to the majority of the trîazi- nes, it holds a special place among these compounds. So the preparation of it w;th a high yield has been one of the main goals in trîazine chenrstry. While the latest method gives a 37 % yield, by the present work the yield in increased to as high as 93 % .