Sol-jel Yöntemi İle Üretilen SrBr2 Katkılı Kalsiyum Fosfat Malzemelerin Mikroyapı ve Mekanik Özelliklerinin İncelenmesi
Bu çalışmada, kalsiyum fosfat esaslı SrBr2 katkılı sentez malzemeleri sol jel yöntemi ile üretilmiştir. Üretilen malzemelerin morfolojik yapısı ve mekanik özellikleri üzerine SrBr2 bileşiğinin etkileri incelenmiştir. Bu amaçlar doğrultusunda, biyogreftlerin morfolojik etkileri FTIR, XRD ve SEM-EDX analizleri ile incelenirken, mekanik özellikleri de sertlik ve basma testleri yapılarak araştırılmıştır. Bütün sentez malzemelerinin üzerine yapılan FTIR ve XRD incelemeleri sonucu, biyogreftler de katkı malzemelerinin kristaliteyi düşürdüğü ve HA(Hidroksiapatit), β-TCP (Beta trikalsiyum fosfat), Ca3(Si3O9), Ca2H4O9P2 faz yapılarını oluşturduğu gözlenmiştir. Ayrıca yapılan SEM-EDX ve mekanik testler sonucu da, bütün sentez malzemelerinde farklı boyutlarda tane yapısının oluştuğu ve SrBr2 katkı malzemelesinin basma mukavemeti ve sertlik değerlerini yükselttiği belirlenmiştir.
Investigation of Microstructure And Mechanical Properties of SrBr2-doped Calcium Phosphate Materials Produced by Sol-Gel Method
In this study, calcium phosphate based SrBr2-doped synthesized materials were produced by sol gelmethod. The effects of SrBr2 compound on the morphological structure and mechanical properties ofthe produced synthesis materials were investigated. For these purposes, the morphological effects ofsynthesis materials were examined by FTIR, XRD and SEM-EDX analyzes and their mechanicalproperties were investigated by hardness and compression tests.As a result of FTIR and XRD investigations on all synthesized materials, it was observed that the additivematerials decreased the crystallinity and formed the HA (Hydroxyapatite), β-TCP (Beta tricalciumphosphate), Ca3(Si3O9), Ca2H4O9P2 phase structures. In addition, as a result of the SEM-EDX andmechanical tests, it has been determined that different sizes of grain structure in all synthesized materialsare formed and SrBr2 additive increase the compressive strength and hardness values.
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