NURAY ÜST, BURCU AKÇA, SALİH ZEKİ ERZENEOĞLU

Dalgaboyu Ayrımlı X-Işını Floresans Spektrometre Ölçüm Sonuçları Üzerine Etki Eden Faktörler Hakkında Bir İnceleme

Bu çalışmada borun işlenmesinden sonraki ürün atığında, farklı kütleler, selüloz oranları ve farklı taramayüzey alanlarının analiz sonuçları üzerine etkisi ve potasyum nitrat (KNO3) numunesinde pres basıncının analizsonuçlarına etkisi incelenmiştir. Çalışmamamızın amacı farklı kütleler, selüloz oranları, pres basıncı ve farklı taramayüzey alanlarının analiz sonuçları üzerine etkisini Dalgaboyu Ayrımlı X-Işını Floresans Spektrometre (WDXRFS)kullanarak belirlemektir.

Anahtar Kelimeler:

bor, Analiz, dalgaboyu ayrımlı x-ışını floresans spektrometre

An Investigation about the Factors Influence on the Wavelength Dispersive X-Ray Fluorescence Spectrometer Measurement Results

In this study, the effect of different masses, cellulose ratios and different scanning surface areas on the analysis results in the product waste after treatment of boron and the effect of press pressing on the analysis results in the potassium nitrate (KNO3) samples were investigated. The aim of our work is determined the effect of different masses, cellulose ratios, press pressing and different scanning surface areas on the analysis results by using the Wavelength Differential X-Ray Fluorescence Spectrometer.

Keywords:

Wavelength Dispersive X-Ray Fluorescence Spectrometer (WDXRFS), analysis, boron,

PDF

___

Akbaba U, Şahin Y, Turkez H, 2011. Element content analysis by WDXRF in pistachios grown under organic and conventional farming regimes for human nutrition and healthy, Fresenius Environmental Bulletin, 20: 1655-1660.
Buhrke, V. E., 1998, Specimen Preparation, Rigaku Journal, 16: 3-5.
Cal-Prieto M.J, Felipe-Sotelo, M, Carlosena, A., Andrade, J.M, López-Mahía, P, Muniategui, S, Prada, D, 2002, Slurry sampling for direct analysis of solid materials by electrothermal atomic absorption spectrometry (ETAAS)= A literature review from 1990 to 2000, Talanta, 56: 1-51.
Fernandes, T A P, Brito, J A A, Goncalves, L M L, 2015, Analysis of Micronutrients and Heavy Metals in Portuguese Infant Milk Powders by WDXRF, Food Analytical Methods, 8: 52-57.
Garivait, S, Quisefit, J.P, Chateaubourg, P, Malingre, G, 1997, Multi-Element Analysis of Plants by WDXRF using Scattered Radiation Correction Method, X-Ray Spectrometry, 26: 257-264.
Hoenig, M, Kersabiec, A.M, 1996, Sample preparation steps for analysis by atomic spectroscopy methods: present status, Spectrochimica Acta Part B: Atomic Spectroscopy, 51, 1297- 1307.
Kubala-Kukus, A, Banas, D, Braziewicz, J, Dziadowicz, M, Kopec, E, Majewska, U, Mazurek, M, Pajek, M, Sobisz, M, Stabrawa, I, 2015, X-ray spectrometry and X-ray microtomography techniques for soil and geological samples analysis, Nuclear Instruments & Methods in Physics Research Section B-Beam Interactions with Materials and Atoms, 364: 85-92.
McWilliams, A.C, Martin, A. A, Levine, M. A, Levine, K. E, Felder, L, Young, D. J, Harrington, J. M, 2015, Preparation of Thin Films for Elemental Analysis of Nail Polish by WDXRFS, Analytical Letters, 48: 2122-2135.
Oliveira, E, 2003. Sample preparation for atomic spectroscopy: evolution and future trends, Journal of the Brazilian Chemical Society, 14, 174-182.
Paulino, A.I; Heldal, M, Norland, S, Egge, J.K, 2013, Elemental stoichiometry of marine particulate matter measured WDXRFS, Journal of the Marine Biological Association of the United Kingdom, 93:2003-2014.
Smolinski, A, Stempin, M, Howaniec, N, 2016, Determination of rare earth elements in combustion ashes from selected Polish coal mines by WDXRFS, Spectrochimica Acta Part B-Atomic Spectroscopy, 116: 63-74.
Teruel, J.D, Alcolea, A, Hernandez, A, Ruiz, A.J.O, 2015, Comparison of chemical composition of enamel and dentine in human, bovine, porcine and ovine teeth, Archives of Oral Biology, 60: 768-775.
Yamini, Y, Amiri, N, Karimi, M, 2009, Determination of trace elements in natural water using X-ray fluorescence spectrometry after preconcentration with powdered silica gel, X-Ray Spectrom., 38: 474-478.